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the solution is cooled to about 1C (-2 to 4C) and p -toluenesulfonyl chloride (1.0 kg) is added and then triethylamine (0.82 kg) at no more than 10C is slowly added (over about 3-6 hours in an exothermic reaction)

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doi: 10.1016/j.brainresbull.2004.02.002 140 MadeiraMDSousaNLima-AndradeMTCalheirosFCadete-LeiteAPaula-BarbosaMM

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